LIU Yang, PEI Jing-qiu, LI Jiang, HE Guo-qiang. Ablation characteristics of a 4D carbon/carbon composite under a high flux of combustion products with a high content of particulate alumina in a solid rocket motor. New Carbon Mater., 2017, 32(2): 144-151. doi: 10.1016/S1872-5805(17)60112-4
Citation: LIU Yang, PEI Jing-qiu, LI Jiang, HE Guo-qiang. Ablation characteristics of a 4D carbon/carbon composite under a high flux of combustion products with a high content of particulate alumina in a solid rocket motor. New Carbon Mater., 2017, 32(2): 144-151. doi: 10.1016/S1872-5805(17)60112-4

Ablation characteristics of a 4D carbon/carbon composite under a high flux of combustion products with a high content of particulate alumina in a solid rocket motor

doi: 10.1016/S1872-5805(17)60112-4
Funds:  National Natural Science Foundation of China (51276150, 51576165); Fundamental Research Funds for the Central Universities (3102014ZD0032).
  • Received Date: 2017-01-27
  • Accepted Date: 2017-04-26
  • Rev Recd Date: 2017-04-09
  • Publish Date: 2017-04-28
  • The ablation behavior of a four-directional carbon/carbon (C/C) composite was examined in a lab-scale solid rocket motor under a high flux of combustion products containing a high content of particulate alumina. The composite consisted of three braided carbon fiber bundles at 120° to each other in the XY plane and a hexagonal array of carbon rods in the Z direction, all in a pitch carbon matrix. The rods consisted of a unidirectional array of the same carbon fibers in a pitch carbon matrix The composite was placed in the rocket motor with its XY plane perpendicular to the gas flow and its ablation rate, ablation behavior and microstructure were investigated. The flow field of the combustion products was simulated by solving the Reynolds-averaged Navier-Stokes equations. A deep pit was formed on the surface of the composite, the center of which coincides with the simulated particle accumulation area. The mechanical erosion was significantly increased when the particle impact velocity exceeded 96.82 m/s. The carbon rods were more susceptible to erosion than the surrounding fiber bundles. The maximum ablation rates of the carbon rod and bundles were increased almost by an order of magnitude by increasing the particle impact velocity by a factor of two. Numerous crater-like pores on the ends of the carbon rods were formed by alumina particle impaction, and the tips of the fibers in the carbon rods were almost flat and lower than the surrounding matrix. Heating caused by the particle impact increased the thermal oxidization and hence the overall ablation rate of the composite.
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  • Liggett N D, Menon S. Simulation of nozzle erosion process in a solid propellant rocket motor[C]. 45th AIAA Aerospace Sciences Meeting and Exhibit, Reno, NV, AIAA Paper: 2007.
    Guiming S, Yu Z, Yujin W, Tingquan L. Throat materials for solid rocket motors[J]. Journal of Solid Rocket Technology. 1998, 2: 12.
    Feng Z, Ruilian Y, Chengzhao Y, et al. Ablative erosion performance of four thermal protection composite materials[J]. Aerospace Materials & Technology, 2001, 31(006): 10-13.
    Yu J, Ma Z, Jiang G, et al. Pattern surface measure and ablation analysis for C/C composite material[J]. Aerospace Materials & Technology, 2003, 33(1): 36-39.
    Andrew C, Eric B, Ragini A, et al. Design of a solid rocket motor for characterization of submerged nozzle erosion[C]. 44th AIAA/ASME/SAE/ASEE Joint Propulsion Conference & Exhibit: American Institute of Aeronautics and Astronautics 2008.
    Wirzberger H, Yaniv S. Prediction of erosion in a solid rocket motor by alumina particles[C]. 41 st AIAA/ASME/SAE/ASEE Joint Propulsion Conference & Exhibit: 1-16.
    Xu X, Huang h. Progress of research in denudation mechanism[J]. Failire analysis and prevention, 2007, 2(3): 59-63.
    Li KZ, Shen XT, Li HJ, et al. Ablation of the carbon/carbon composite nozzle-throats in a small solid rocket motor[J]. Carbon, 2011, 49(4): 1208-1215.
    Chen B, Zhang LT, Cheng LF, et al. Erosion resistance of needled carbon/carbon composites exposed to solid rocket motor plumes[J]. Carbon, 2009, 47(6): 1474-1479.
    Sarkar S, Sekharan VG, Mitra R, et al. The solid particle erosion behavior of carbon/carbon and carbon/phenolic composite used in re-entry vehicles[J]. Tribol T, 2009, 52(6): 777-787.
    Oka YI, Okamura K, Yoshida T. Practical estimation of erosion damage caused by solid particle impact - Part 1: Effects of impact parameters on a predictive equation[J]. Wear, 2005, 259(1-6): 95-101.
    Thakre P, Rawat R, Clayton R, et al. Mechanical erosion of graphite nozzle in solid-propellant rocket motor[J]. J Propul Power, 2013, 29(3): 593-601.
    Li Q, Li J, He GQ, et al. Erosion of carbon/carbon composites using a low-velocity, high-particle-concentration two-phase jet in a solid rocket motor[J]. Carbon, 2014, 67: 140-145.
    Peng LN, He GQ, Li J, et al. Effect of combustion gas mass flow rate on carbon/carbon composite nozzle ablation in a solid rocket motor[J]. Carbon, 2012, 50(4): 1554-1562.
    Gordon S, Mcbride B. Computer program for calculation of complex chemical equilibrium compositions and applications. Part 1: Analysis[Z]. 1994.
    McBride B J, Gordon S. Computer program for calculation of complex chemical equilibrium compositions and applications: II. Users' manual and program description[Z]. NASA reference publication, 1996, 1311: 84-85.
    Glorieux B, Millot F, Rifflet J-C,et al. Density of superheated and undercooled liquid alumina by a contactless method[J]. International journal of Thermophysics, 1999, 20(4): 1085-1094.
    Sinn H, Glorieux B, Hennet L, et al. Microscopic dynamics of liquid aluminum oxide[J]. Science, 2003, 299(5615): 2047-2049.
    Liu Y. The experimental simulation technique of flow field under high acceleration condition[D]. Xi'an: Northwestern Polytechnical University, Master thesis, 2004.
    Cortopassi A C, Boyer E, Kuo K K. Update: a subscale solid rocket motor for characterization of submerged nozzle erosion[C]. 45th AIAA/ASME/SAE/ASEE Joint Propulsion Conference & Exhibit, Joint Propulsion Conferences, 2009, 5172: 2009.
    Li Q, He G Q, Liu P J, et al. Coupled simulation of fluid flow and propellant burning surface regression in a solid rocket motor[J]. Comput Fluids, 2014, 93: 146-152.
    Zhang X, Liu P, Li P, et al. Heat flux measurement method and experimental research in SRM[J]. Journal of Solid Rocket Technology, 2011, 34(1): 131-134.
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