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Recent progress in the use of graphene/polymer composites to remove oil contaminants from water

FENG Zhao-xuan XU Ya-nan YUE Wei-xun Karin H. Adolfsson WU Ming-bo

冯昭璇, 徐亚男, 岳维勋, Karin H.Adolfsson, 吴明铂. 石墨烯/聚合物纳米复合材料去除水中废油污染物的研究进展[J]. 新型炭材料, 2021, 36(2): 235-252. doi: 10.1016/S1872-5805(21)60023-19
引用本文: 冯昭璇, 徐亚男, 岳维勋, Karin H.Adolfsson, 吴明铂. 石墨烯/聚合物纳米复合材料去除水中废油污染物的研究进展[J]. 新型炭材料, 2021, 36(2): 235-252. doi: 10.1016/S1872-5805(21)60023-19
FENG Zhao-xuan, XU Ya-nan, YUE Wei-xun, Karin H. Adolfsson, WU Ming-bo. Recent progress in the use of graphene/polymer composites to remove oil contaminants from water[J]. NEW CARBOM MATERIALS, 2021, 36(2): 235-252. doi: 10.1016/S1872-5805(21)60023-19
Citation: FENG Zhao-xuan, XU Ya-nan, YUE Wei-xun, Karin H. Adolfsson, WU Ming-bo. Recent progress in the use of graphene/polymer composites to remove oil contaminants from water[J]. NEW CARBOM MATERIALS, 2021, 36(2): 235-252. doi: 10.1016/S1872-5805(21)60023-19

石墨烯/聚合物纳米复合材料去除水中废油污染物的研究进展

doi: 10.1016/S1872-5805(21)60023-19
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  • 中图分类号: TB33

Recent progress in the use of graphene/polymer composites to remove oil contaminants from water

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  • 摘要: 频繁的海上溢油事故和工业含油污水的肆意排放严重破坏海洋生态平衡。因此,开发先进的除油材料迫在眉睫。石墨烯(G)及其衍生物氧化石墨烯(GO)因其具有高比表面积、低密度、高孔隙率、表面功能可调等优异的理化性质,在油水分离领域成为研究热点。为充分发挥其优势,近年来,将G或GO与聚合物复合制备成功能化G/聚合物或GO/聚合物纳米复合材料,因其具有良好的除油能力、优异的机械性能、价格低廉、形貌及表面化学组分可调等优势而越来越受到人们的青睐。目前已开发出气凝胶、泡沫、海绵、膜等具有三维结构的G/聚合物或GO/聚合物复合吸油剂和过滤膜。本文系统性地总结了从表面润湿理论到G/聚合物或GO/聚合物复合吸油材料和滤膜材料的最新研究进展。此外,重点归纳了近年来有关油品回收及吸油材料再生的方法策略。最后,提出该研究领域目前面临的挑战和未来研究方向,旨在为该领域的深入探索开辟新的视角。
  • FIG. 566.  FIG. 566.

    FIG. 566.. 

    Figure  1.  (a) A schematic illustration showing how to measure the contact angle, (b) a schematic illustration of the Wenzel model and (c) a schematic illustration of the Cassie model.

    Figure  2.  (a) Absorption process of AG-1 towards paraffin oil(Sudan red-stained paraffin oil floating on water was completely absorbed within 62 s, (b) absorption capacities of AG-1 (black) and AG-2 (red) towards various oils and common organic solvents (adapted from Ref[51] with permission. Copyright 2014 The Royal Society of Chemistry), (c) a schematic illustration showing the fabrication procedure of CNF/PVA/GO composite aerogels, (d1) photographs of d-MCPGAby freeze-drying methods, (d2) SEM image showing the vertical section of d-MCPGA, (d3) SEM image showing the cross section of d-MCPGA, (e) water contact angles of d-MCPGA measured from 0 s to 120 s, (f) absorption capacities of MCPGA (d-MCPGA, r-MCPGA, n-MCPGA) for various types of oils and organic solvents, (g1) photograph showing the ultra-light cylindrical d-MCPGA hold up by the young leaves, (g2) the shape of the d-MCPGA before bearing 500 g mass load, (g3) the shape of the d-MCPGA after bearing 500 g mass load and (g4) the state of d-MCPGA when bearing 500 g mass load. (adapted from Ref[56] with permission (Copyright 2019 Multidisciplinary Digital Publishing Institute).

    Figure  3.  (a) SEM image of a cellulose nanofibrous foam, (b) physical appearance of the cellulose nanofibrous foam, (c,e) SEM images of a cellulose nanofibrous aerogel at different magnifications and (d) physical appearance of the cellulose nanofibrous aerogel. (adapted from Ref[78] with permission. Copyright 2016 PubMed)

    Figure  4.  (a) The oil and solvent absorption capacities of G/PPy, (b) cyclic absorption capacities of G/PPy foam towards diesel (adapted from Ref[59] with permission. Copyright 2013 The Royal Society of Chemistry), (c) photographs and a schematic illustration showing the fabrication of the rGO@PU foam, (d) absorption capacity of the neat PU and rGO@PU foams towards oils and organic solvents, (e) cyclic absorption capacities of the rGO@PU foam towards oils and organic solvent and (f) oil-removing efficiency of the rGO@PU foam (adapted from Ref[60]with permission. Copyright 2018 Elsevier).

    Figure  5.  (a) Oil/water separation capacities of GO/PES composite flat sheet (FS) and hollow fiber (HF) membranes at different oil concentrations (adapted from Ref[85]with permission. Copyright 2020 Wiley), (b) a schematic illustration showing the preparation procedure of the GO-Ca2+-SA hybrid mesh by layer-by-layer self-assembly and cross-linking (adapted from Ref[91]with permission. Copyright 2020 Elsevier), (c) TEM image of the hybrid membrane with 7 wt% of GO, (left), the magnified TEM image of the spindle-knot structure (middle), the magnified TEM image of PAN and GO sheets (right), (d) relation curves between flux and permeation volume of PAN/GO membranes (left), relation curves between flux and permeation volume of H-PAN/GO membranes (inset was permeation volume = 200 mL) (right) (adapted from Ref[89] with permission. Copyright 2017 Elsevier) and (e) functionalization of GO with aspartic acid (adapted from Ref[90]with permission. Copyright 2017 Elsevier).

    Figure  6.  (a) A schematic illustration showing the fabrication procedure of CGQD-incorporated ENCF membrane, (b) toluene permeation flux of the CGQD-incorporated ENCF membrane with various concentrations of CGQD, (c) the permeation flux of the CGQD-incorporated ENCF membrane to several common organic solvents (adapted from Ref[97] with permission. Copyright 2018 Elsevier).

    Table  1.   The synthetic methods, WCA and oil absorption capacities of G/polymer and GO/polymer composite aerogels and foams.

    MaterialSynthesis methodWater contact angleOil absorption
    capacity (g/g)
    Number of cycleRef.
    G/PVDF aerogelsSolvothermal reduction153.6°20−7010[51]
    PI-GO aerogelSupercritical drying-8.0-[52]
    LGA aerogelsHydrothermal treatment and freeze-drying127°167−35010[54]
    G/CNC aerogelLyophilize andcoating130°25−58100[55]
    CNF/PVA/GO aerogelDirectional freeze-drying technology and hydrophobic treatment142°60−96-[56]
    XPAA/rGO aerogelVacuum heated-120-[57]
    a-GPCCA aerogelDirectional freeze-drying and carbonization140°155−28815[58]
    G/PPy foamsHydrothermal method and vacuum freeze Dried->10011[59]
    rGO@PU foamSolvothermal method153°3750[60]
    G/PU foam-158°700200[61]
    LPU-rGO-ODAfoamDried in air152°26−2820[62]
    PEI/GO foamDried at 60 °C-17>3[63]
    PDMS/GO spongeAmidation reaction and drying under vacuum174.1 ± 0.6 °14.610[64]
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出版历程
  • 收稿日期:  2021-02-17
  • 修回日期:  2021-03-16
  • 网络出版日期:  2021-03-31
  • 刊出日期:  2021-04-01

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