Volume 38 Issue 6
Nov.  2023
Turn off MathJax
Article Contents
JIA Lin-tao, WANG Meng-qian, GUO Xiao-feng, ZHU Jie, LI Ai-jun, PENG Yu-qing. Effect of chemical vapor infiltration on the flexural properties of C/C-SiC composites prepared by the precursor infiltration pyrolysis method. New Carbon Mater., 2023, 38(6): 1127-1134. doi: 10.1016/S1872-5805(23)60732-2
Citation: JIA Lin-tao, WANG Meng-qian, GUO Xiao-feng, ZHU Jie, LI Ai-jun, PENG Yu-qing. Effect of chemical vapor infiltration on the flexural properties of C/C-SiC composites prepared by the precursor infiltration pyrolysis method. New Carbon Mater., 2023, 38(6): 1127-1134. doi: 10.1016/S1872-5805(23)60732-2

Effect of chemical vapor infiltration on the flexural properties of C/C-SiC composites prepared by the precursor infiltration pyrolysis method

doi: 10.1016/S1872-5805(23)60732-2
Funds:  National Natural Science Foundation of China (21676163, 51602189),Aeronautical Science Foundation of China (2016ZFS6001,2017ZFS6001) and The Shanghai Natural Science Fund (No. 18ZR1417700)
More Information
  • Author Bio:

    贾林涛,博士研究生. E-mail:jia0721@shu.edu.cn

  • Corresponding author: LI Ai-jun, Professor. E-mail: aijun.li@shu.edu.cn
  • Received Date: 2020-02-20
  • Rev Recd Date: 2020-08-24
  • Available Online: 2023-03-13
  • Publish Date: 2023-11-23
  • Carbon/carbon-silicon carbide (C/C-SiC) composites were prepared by impregnation, hot-pressing with curing, carbonization at 800 oC and high-temperature heat treatment (800-1600 oC) using a 2D laminated carbon cloth as the reinforcing filler, and furfurone resin mixed with silicon, carbon from furfurone resin and SiC powders as the matrix. The effects of the addition of the three powders as well as subsequent chemical vapor infiltration (CVI) by methane on the density, microstructure and bend strength of the composites were investigated by scanning electron microscopy, density measurements, X-ray diffraction and mechanical testing. Both the SiC powders formed by the reaction at 1600 oC between the added Si and C particles and the added SiC powder, play a role in the reinforcement of the materials. In three-point bending, the composites had a pseudoplastic fracture mode and showed interlaminar cracking. After 10 h CVI with methane, pyrolytic carbon was formed at the interface between some of the carbon fibers and the resin carbon matrix, which produced maximum increases in the density and flexural strength of the composites of 4.98% and 38.86%, respectively.
  • loading
  • [1]
    Qiu M, Hang Y, Liu Z, et al. A review of the fabrication methods for solar silicon wafer[J]. Mechanical Science and Technology for Aerospace Engineering,2008(08):43-46.6.
    [2]
    Quan C. Preparation and Passivation of Silicon Nitride Thin Films for Solar Cells[M]. University of Electronic Science and Technology of China, 2012.
    [3]
    Gorin A, Jaouad A, Grondin E, et al. Fabrication of silicon nitride waveguides for visible-light using PECVD: A study of the effect of plasma frequency on optical properties[J]. Optics Express,2008,16(18):13509-16. doi: 10.1364/OE.16.013509
    [4]
    Zhou Z, Cai X, Liu W. Preparation of silicon nitride thin films for solar cells by PECVD[J]. Solar Energy,2017,8:43-47.
    [5]
    Zhang B, Dang J. Graphite boat pin and coating device[P]. CN 207130336 U. 2018.
    [6]
    Bai X, Guo W, Jia Y, et al. Study on the uniformity of polycrystalline PECVD coating[J]. Technological Development of Enterprise,2013,32(Z2):51-52+54.54.
    [7]
    Fu Q, Li H, Shen X, et al. Domestic research process of matrix modification for carbon/carbon composites[J]. Materials China,2011,30(11):6-12.
    [8]
    Su J, Li Y, Xiao Z, et al. Preparation and properties of the U-shaped carbon-carbon composite radiator[J]. Carbon,2011,1:21-24.
    [9]
    Li T, Yang Z, Zheng X, et al. The relationship between the surface state of carbon fiber and the ILSS of C/C composites[J]. Ordnance Material Science and Engineering,1993,04:8-11.
    [10]
    Li C, Zheng J, Su H, et al. Mechanical and thermophysical properties of two dimensional carbon/carbon composites at elevated temperatures[J]. Aerospace Materials & Technology,2004,34(1):33-37.
    [11]
    Jian K, Hu H, Chen Z. Fabrication of low-cost C/SiC composite from silicon powder and phenolic resins[J]. Development and Application of Materials,2002,17(6):12-14.
    [12]
    Yan L, Li H, Cui H, et al. C/SiC composites prepared by inner siliconizing process[J]. Journal of Materials Engineering,2005(09):41-44+52.
    [13]
    Wang M. Application of carbon fiber composites in aerospace field[J]. Modern Business Trade Industry,2019,40(08):195-197.
    [14]
    Hu L, Li C, Zhang Y. Influence of C/C thermal treatment temperature on microstructure and thermal properties of C/C-SiC composites[J]. Carbon,2018(1):18-23.
    [15]
    Xia L, Zhang H, Xiong X, et al. Curing reaction of furfural acetone resin used for new carbon materials[J]. The Chinese Journal of Nonferrous Metals,2008(06):7-12.
    [16]
    Wang J, Guo L, Li H, et al. Curing, characteristics and kinetic analysis of furfural acetone resin used as carbon /carbon composites precursor[J]. Journal of Solid Rocket Technology,2012,35(01):127-130+136.
    [17]
    Donh L, Zhang B, Tian J, et al. Study on the oxidation resistance of carbon ceramic composites[J]. Journal of Tsinghua University (Science and Technology),1997,37(05):108-111.
    [18]
    Chollion G, Siron O, Takahashi J, et al. Microstructure and mechanical properties of coal tar pitch-based 2D-C/C composites with a filler addition[J]. Carbon,2001,39(13):2065-2075. doi: 10.1016/S0008-6223(01)00021-5
    [19]
    Peng X, Zhuan L, Xiang X. Manufacture and tribological properties of C/C-SiC brake composites fabricated by warm compacted in situ reaction[J]. Tribology,2012(04):332-337.
    [20]
    Mikociak D, Rudawski A, Blazewicz S. Mechanical and thermal properties of C/C composites modified with SiC nanofiller[J]. Materials Science and Engineering:A,2018,716:220-227. doi: 10.1016/j.msea.2018.01.048
    [21]
    Qin M, Xiao P, Xiong X, et al. Mechanical properties of C/C-SiC composites prepared with different phenolic resin[J]. Materials Science and Engineering of Powder Metallurgy,2008,13(06):346-351.
    [22]
    Zhou S, Wu X, Cui H, et al. Influence of graphite filler on the performance of C/C-SiC composites based on LSI[J]. Journal of Solid Rocket Technology,2015,38(02):281-285.
    [23]
    Zhao W, Zhu B, Shi Z, et al. Study on moulding process and properties of C/C-SiC composites[J]. Journal of Functional Materials,2015,46(S1):152-155.
    [24]
    Schulte-Fischedick J, Frieß M, Krenkel W, et al. The interlaminar shear strength of C/C-SiC[J]. High Temperature Ceramic Matrix Composites,2001:181-186.
    [25]
    Chen Z, Zhang L, Cheng L, et al. Preparation of C fiber reinforced alumina-mullite composite by PIP and CVI[J]. Journal of Inorganic Materials,2003,18(3):638-644.
    [26]
    Li C, Ma B, Jin Z. The fracture toughness of 2D carbon-carbon composite[J]. Journal of Solid Rocket Technology,2003,26(1):67-70.
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(14)  / Tables(1)

    Article Metrics

    Article Views(262) PDF Downloads(100) Cited by()
    Proportional views
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return