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摘要: 利用Weibull统计分布分析了上浆对炭纤维单丝拉伸强度的影响。通过扫描电镜(SEM)观察和X射线能谱仪(EDS)分析了上浆前后炭纤维表面和截面的结构形貌及表面元素组成。结果表明:当纳米SiO2粒子与上浆树脂的质量比为0.5%时,上浆炭纤维单丝的抗拉强度最高,增幅达10.1%;Weibull参数m值最大,强度的分散性最小。EDS显示了改性上浆炭纤维表面Si元素含量增大。上浆炭纤维比未上浆的表面较均匀,纹理沟槽变浅;截面凹凸不平,呈现一定的韧性断裂特性。说明上浆剂中添加纳米SiO2粒子可以明显提高上浆炭纤维的强度。Abstract: The influence of a nanoSiO2 modified sizing on the tensile strength of carbon fibers was studied by SEM and Xray energy dispersion spectrum tester (EDS). The tensile strength of the resulting carbon fibers was analyzed by the Weibull method. Results showed that when the ratio of SiO2 nanoparticles to epoxy resin was 0.5 w/%,the fiber strength reached a maximum value, 10.1% larger than that of the unsized carbon fibers, and the Weibull parameter exhibited a maximum, indicating a minimum distribution of tensile strength. EDS indicated that the content of elemental Si increased on the surfaces of the sized carbon fibers with nanoSiO2/epoxy emulsion. The sized fibers surfaces were even and the surface grooves were shallow, compared to unsized fibers. However, the fracture crosssections of the sized fibers were concave or convex, indicating a tough fracture character.
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Key words:
- Carbon fibers /
- NanoSiO2 /
- Sizing /
- Weibull
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