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摘要: 采用 3 种不同粒径的纳米金刚石与树脂基体、光固化剂和其他填料复合,合成光固化复合树脂。 探讨纳米金刚石对光固化复合树脂挠曲强度、固化深度等性能的作用规律。 结果表明,纳米金刚石可显著地增强树脂的挠曲强度、弹性模量等机械性能,但也会降低树脂的固化深度。 发现纳米金刚石对光固化复合树脂的增强作用中存在逾渗现象,即当纳米金刚石含量达到一定数值后会导致树脂的机械性能明显降低。 性能最佳的光固化复合树脂应该选择粒径为 220 nm 的纳米金刚石,其添加量在 0. 15% 左右为宜。Abstract: Light-cured composite resins were prepared by illuminating a cylinder with a diameter of 4 mm and a length of 6 mm for 40 s, using bisphenol A ethoxylate dimethacrylate as monomer, triethyleneglycol dimethacrylate as diluting agent, camphoroqui-none and dimethyaminoethyl methacrylate as photoinitiators and nanodiamonds as reinforcements. The nanodiamonds were of different size and were surface-modified by methacryloxypropyltrimethoxy silane. The flexural strength, elastic modulus and other mechanical properties of the resins were investigated to determine how the nanodiamonds influenced the properties of the composite res ins. Results showed that the nanodiamonds significantly improved flexural strength and elastic modulus of the composite resins, but also decreased their depth of lightcuring. A percolation phenomenon was found in the composite resins, which indicated that their mechanical properties decreased significantly when the nanodiamond content was greater than a value depend
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Key words:
- Nanodiamond /
- Light-curing /
- Composite resin /
- Percolation /
- Reinforce
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