利用感应加热技术进行炭纤维连续石墨化

利用感应加热技术进行炭纤维连续石墨化

  • 摘要: 采用感应加热技术研制出炭纤维连续高温热处理专用设备石墨化炉,最高使用温度3000℃。对PAN基炭纤维T300进行了连续石墨化处理,热处理温度为2000℃~3000℃,制备出力学性能相当于日本东丽公司M40的石墨纤维,验证了该设备的技术可行性。考察了热处理温度对炭纤维力学性能、密度和直径的影响,用SEM观察了石墨化前后炭纤维表面微观形态的变化。结果表明:随热处理温度的提高,炭纤维的密度增大、直径减小,弹性模量升高,而抗拉强度下降。经3000℃高温热处理后,纤维的弹性模量高达450GPa。

     

    Abstract: Large isotropic pyrolytic carbon rings were fabricated by a steady fluidized bed deposition apparatus with a rotating substrate. The microstructure of the isotropic pyrolytic carbons obtained was investigated by polarized light microscopy, SEM, TEM and XRD. Their mechanical properties were also studied. Observations using polarized light microscopy and SEM show that the microstructure is homogeneous and there is a small amount of closed porosity inside. TEM observations show that this material is mainly made up of fine turbostratic carbon structures. Mechanical tests show that the Young’s modulus, microhardness, flexural strength and compressive strength of the carbons are higher than those of traditional carbon materials.

     

/

返回文章
返回